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1

Formation of ( S )-5-Cyclohexyl-5-phenyl-1,3-dioxolane-2,4-dione: A Key Intermediate in the Synthesis of ( S )-Oxybutynin Hydrochloride †

Vandenbossche, Charles P., de Croos, Philomen, Singh, Surendra P., Bakale, Roger P., Wagler, Thomas R.

Journal:

Organic Process Research & Development

Year:

2010

Language:

english

File:

PDF, 267 KB

english, 2010

2

An Efficient Synthesis of Enamides from Ketones

Zhao, Hang, Vandenbossche, Charles P., Koenig, Stefan G., Singh, Surendra P., Bakale, Roger P.

Journal:

Organic Letters

Year:

2008

Language:

english

File:

PDF, 68 KB

english, 2008

3

Development of a Process Route to the FAK/ALK Dual Inhibitor TEV-37440

Allwein, Shawn, Mowrey, Dale R, Petrillo, Daniel, Reif, James, PUROHIT, VIKRAM C, Milkiewicz, Karen, Bakale, Roger, Christie, Michael, Olsen, Mark, Neville, Christopher, Gilmartin, Gregory

Journal:

Organic Process Research & Development

Year:

2017

Language:

english

File:

PDF, 368 KB

english, 2017

4

ChemInform Abstract: Rigid Aminoalcohol Backbone as a Highly Defined Chiral Template for the Preparation of Optically Active Tertiary α-Hydroxyl Acids.

Chris H. Senanayake, Kevin Fang, Paul Grover, Roger P. Bakale, Charles P. Vandenbossche, Stephen A. Wald

Journal:

Year:

1999

File:

PDF, 37 KB

1999

5

ChemInform Abstract: Properly Tuned First Fluoride-Catalyzed TGME-Mediated Amination Process for Chloroimidazoles: Inexpensive Technology for Antihistaminic Norastemizole.

Chris H. Senanayake, Yaping Hong, Tingjian Xiang, H. Scott Wilkinson, Roger P. Bakale, Alex R. Jurgens, Mark F. Pippert, Hal T. Butler, Stephen A. Wald

Journal:

Year:

1999

File:

PDF, 31 KB

1999

6

ChemInform Abstract: A New Lithium Alkoxide Accelerated Diastereoselective Cyanation of Ketones.

H. Scott Wilkinson, Paul T. Grover, Charles P. Vandenbossche, Roger P. Bakale, Nandkumar N. Bhongle, Stephen A. Wald, Chris H. Senanayake

Journal:

Year:

2001

File:

PDF, 31 KB

2001

7

Efficient and Scalable Arylation of Bicyclic Lactones to Form Quaternary Centers Using Conventional and Microwave Radiation.

Scott C. Malcolm, Seth Ribe, Fengjiang Wang, Michael C. Hewitt, Nandkumar Bhongle, Roger P. Bakale, Liming Shao

Journal:

Year:

2006

File:

PDF, 22 KB

2006

8

ChemInform Abstract: A Facile Deprotection of Secondary Acetamides.

Stefan G. Koening, Charles P. Vandenbossche, Hang Zhao, Patrick Mousaw, Surendra P. Singh, Roger P. Bakale

Journal:

Year:

2009

File:

PDF, 33 KB

2009

9

The pilot plant real book—‘a unique handbook for the chemical process industry’. By Francis X McConville, FXM Engineering and Design, 2002. ISBN 0 9721769 1 8

Journal:

Journal of Chemical Technology & Biotechnology

Year:

2004

Language:

english

File:

PDF, 35 KB

english, 2004

10

In vitro and in vivo evaluation of O-alkyl derivatives of tramadol

Liming Shao, Michael Hewitt, Thomas P. Jerussi, Frank Wu, Scott Malcolm, Paul Grover, Kevin Fang, Patrick Koch, Chris Senanayake, Nandkumar Bhongle, Seth Ribe, Roger Bakale, Mark Currie

Journal:

Bioorganic & Medicinal Chemistry Letters

Year:

2008

Language:

english

File:

PDF, 163 KB

english, 2008

11

Factors affecting on-line estimation of diastereomer composition using Raman spectroscopy

Sze-Wing Wong, Christos Georgakis, Gregory Botsaris, Kostas Saranteas, Roger Bakale

Journal:

Control Engineering Practice

Year:

2007

Language:

english

File:

PDF, 931 KB

english, 2007

12

A large-scale asymmetric synthesis of (S)-cyclohexylphenyl glycolic acid

Xiping Su, Nandkumar N Bhongle, Derek Pflum, Hal Butler, Stephen A Wald, Roger P Bakale, Chris H Senanayake

Journal:

Tetrahedron: Asymmetry

Year:

2003

Language:

english

File:

PDF, 212 KB

english, 2003

13

Efficient and scalable arylation of bicyclic lactones to form quaternary centers using conventional and microwave radiation

Scott C. Malcolm, Seth Ribe, Fengjiang Wang, Michael C. Hewitt, Nandkumar Bhongle, Roger P. Bakale, Liming Shao

Journal:

Tetrahedron Letters

Year:

2005

Language:

english

File:

PDF, 94 KB

english, 2005

14

Palladium catalyzed amination of 2-chloro-1,3-azole derivatives: Mild entry to potent H1- antihistaminic norastemizole

Yaping Hong, Gerald J. Tanoury, H.Scott Wilkinson, Roger P. Bakale, Stephen A. Wald, Chris H. Senanayake

Journal:

Tetrahedron Letters

Year:

1997

Language:

english

File:

PDF, 272 KB

english, 1997

15

Rigid aminoalcohol backbone as a highly defined chiral template for the preparation of optically active tertiary α-hydroxyl acids

Chris H. Senanayake, Kevin Fang, Paul Grover, Roger P. Bakale, Charles P. Vandenbossche, Stephen A. Wald

Journal:

Tetrahedron Letters

Year:

1999

Language:

english

File:

PDF, 279 KB

english, 1999

16

Properly tuned first fluoride-catalyzed TGME-mediated amination process for chloroimidazoles: inexpensive technology for antihistaminic norastemizole

Chris H. Senanayake, Yaping Hong, Tingjian Xiang, H.Scott Wilkinson, Roger P. Bakale, Alex R. Jurgens, Mark F. Pippert, Hal T. Butler, Stephen A. Wald

Journal:

Tetrahedron Letters

Year:

1999

Language:

english

File:

PDF, 306 KB

english, 1999

17

Synthesis of enantiomerically pure desmethylzopiclone and determination of its absolute configuration

Yaping Hong, Roger P. Bakale, Qun K. Fang, Tingjian Xiang, Zhengxu Han, Fran X. McConville, Chris H. Senanayake, Stephen A. Wald

Journal:

Tetrahedron: Asymmetry

Year:

2000

Language:

english

File:

PDF, 232 KB

english, 2000

18

Remarkably selective palladium-catalyzed amination process: Rapid assembly of multiamino based structures

Yaping Hong, Chris H. Senanayake, Tingjian Xiang, Charles P. Vandenbossche, Gerald J. Tanoury, Roger P. Bakale, Stephen A. Wald

Journal:

Tetrahedron Letters

Year:

1998

Language:

english

File:

PDF, 238 KB

english, 1998

19

ChemInform Abstract: A General Preparation of Protected Phosphoamino Acids.

Daniel E. Petrillo, Dale R. Mowrey, Shawn P. Allwein, Roger P. Bakale

Journal:

Year:

2012

File:

PDF, 31 KB

2012

20

Albuterol

Roger P. Bakale, Stephen A. Wald, Hal T. Butler, Yun Gao, Yaping Hong, Xiaoyi Nie, Charles M. Zepp

Journal:

Clinical Reviews in Allergy & Immunology

Year:

1996

Language:

english

File:

PDF, 1.38 MB

english, 1996

21

Demonstration of a Scalable One-Pot Synthesis of Fmoc- O -Benzylphospho- l -serine

Mowrey, Dale R., Petrillo, Daniel E., Allwein, Shawn P., Graf, Stéphanie, Bakale, Roger P.

Journal:

Organic Process Research & Development

Year:

2012

Language:

english

File:

PDF, 226 KB

english, 2012

22

Discovery of a Novel, Efficient, and Scalable Route to Bendamustine Hydrochloride: The API in Treanda

Chen, Jian, Przyuski, Katrin, Roemmele, Renee, Bakale, Roger P.

Journal:

Organic Process Research & Development

Year:

2011

Language:

english

File:

PDF, 972 KB

english, 2011

23

Development and Scale-Up of an Optimized Route to the ALK Inhibitor CEP-28122

Allwein, Shawn P., Roemmele, Renee C., Haley, James J., Mowrey, Dale R., Petrillo, Daniel E., Reif, James J., Gingrich, Diane E., Bakale, Roger P.

Journal:

Organic Process Research & Development

Year:

2012

Language:

english

File:

PDF, 503 KB

english, 2012

24

Catalytic Oxidative 1,2-Shift in 1,1′-Disubstituted Olefins Using Arene(iodo)sulfonic Acid as the Precatalyst and Oxone as the Oxidant

Purohit, Vikram C., Allwein, Shawn P., Bakale, Roger P.

Journal:

Organic Letters

Year:

2013

Language:

english

File:

PDF, 400 KB

english, 2013

25

Development of a Large-Scale Stereoselective Process for (1 R ,4 S )-4-(3,4-Dichlorophenyl)-1,2,3,4-tetrahydronaphthalen-1-amine Hydrochloride

Han, Zhengxu, Koenig, Stefan G., Zhao, Hang, Su, Xiping, Singh, Surendra P., Bakale, Roger P.

Journal:

Organic Process Research & Development

Year:

2007

Language:

english

File:

PDF, 80 KB

english, 2007

26

Development and Scale-Up of an Optimized Route to the Pyridazin-3-one Histamine H3 Receptor Antagonist CEP-32215

Wang, Yi, Przyuski, Katrin, Roemmele, Renee C., Hudkins, Robert L., Bakale, Roger P.

Journal:

Organic Process Research & Development

Year:

2013

Language:

english

File:

PDF, 379 KB

english, 2013

27

Discovery and Process Synthesis of Novel 2,7-Pyrrolo[2,1- f ][1,2,4]triazines

Thieu, Tho, Sclafani, Joseph A., Levy, Daniel V., McLean, Andrew, Breslin, Henry J., Ott, Gregory R., Bakale, Roger P., Dorsey, Bruce D.

Journal:

Organic Letters

Year:

2011

Language:

english

File:

PDF, 793 KB

english, 2011

28

A Facile Deprotection of Secondary Acetamides

Koenig, Stefan G., Vandenbossche, Charles P., Zhao, Hang, Mousaw, Patrick, Singh, Surendra P., Bakale, Roger P.

Journal:

Organic Letters

Year:

2009

Language:

english

File:

PDF, 102 KB

english, 2009

29

Improved Continuous Flow Processing: Benzimidazole Ring Formation via Catalytic Hydrogenation of an Aromatic Nitro Compound

Chen, Jian, Przyuski, Katrin, Roemmele, Renee, Bakale, Roger P.

Journal:

Organic Process Research & Development

Year:

2014

Language:

english

File:

PDF, 1.31 MB

english, 2014

30

Tin-directed Baeyer-Villiger and Beckmann fragmentations

Bakale, Roger P., Scialdone, Mark A., Johnson, Carl R.

Journal:

Journal of the American Chemical Society

Year:

1990

Language:

english

File:

PDF, 361 KB

english, 1990

31

Online Estimation and Monitoring of Diastereomeric Resolution Using FBRM, ATR-FTIR, and Raman Spectroscopy

Wong, Sze-Wing, Georgakis, Christos, Botsaris, Gregory D., Saranteas, Kostas, Bakale, Roger

Journal:

Industrial & Engineering Chemistry Research

Year:

2008

Language:

english

File:

PDF, 2.48 MB

english, 2008

32

Informations

Spies, James B., Bakal, Curt W., Burke, Dana R., Cardella, John F., Dawson, Steven L., Drooz, Alain T., Palestrant, Aubrey M., Pentecost, Michael J., Roberts, Anne C., Rogers, William F., Sacks, David

Journal:

Motricité Cérébrale : Réadaptation, Neurologie du Développement

Year:

2008

Language:

french

File:

PDF, 75 KB

french, 2008

33

Standard for Diagnostic Arteriography in Adults

Spies, James B., Bakal, Curt W., Burke, Dana R., Cardella, John F., Dawson, Steven L., Drooz, Alain T., Palestrant, Aubrey M., Pentecost, Michael J., Roberts, Anne C., Rogers, William F., Sacks, David

Journal:

Journal of Vascular and Interventional Radiology

Year:

1993

Language:

english

File:

PDF, 1.15 MB

english, 1993

34

Control of Diastereoselectivity by Solvent Effects in the Addition of Grignard Reagents to Enantiopure t -Butylsulfinimine: Syntheses of the Stereoisomers of the Hydroxyl Derivatives of Sibutramine

Lu, Bruce Z., Senanayake, Chris, Li, Nansheng, Han, Zhengxu, Bakale, Roger P., Wald, Stephen A.

Journal:

Organic Letters

Year:

2005

Language:

english

File:

PDF, 87 KB

english, 2005

35

A New Lithium Alkoxide Accelerated Diastereoselective Cyanation of Ketones

Wilkinson, H. Scott, Grover, Paul T., Vandenbossche, Charles P., Bakale, Roger P., Bhongle, Nandkumar N., Wald, Stephen A., Senanayake, Chris H.

Journal:

Organic Letters

Year:

2001

Language:

english

File:

PDF, 62 KB

english, 2001

36

Online Estimation of Diastereomer Composition Using Raman: Differentiation in High and Low Slurry Density Partial Least Square Models

Wong, Sze-Wing, Georgakis, Christos, Botsaris, Gregory D., Saranteas, Kostas, Bakale, Roger

Journal:

Crystal Growth & Design

Year:

2008

Language:

english

File:

PDF, 2.00 MB

english, 2008

37

A General Preparation of Protected Phosphoamino Acids

Petrillo, Daniel E., Mowrey, Dale R., Allwein, Shawn P., Bakale, Roger P.

Journal:

Organic Letters

Year:

2012

Language:

english

File:

PDF, 222 KB

english, 2012

38

Process Design and Scale-Up Elements for Solvent Mediated Polymorphic Controlled Tecastemizole Crystallization

Saranteas, Kostas, Bakale, Roger, Hong, Yaping, Luong, Hoa, Foroughi, Reza, Wald, Stephen

Journal:

Organic Process Research & Development

Year:

2005

Language:

english

File:

PDF, 870 KB

english, 2005

39

FACTORS AFFECTING ON-LINE ESTIMATION OF DIASTEREOMER COMPOSITION USING RAMAN SPECTROSCOPY

Wong, Sze-Wing, Georgakis, Christos, Botsaris, Gregory, Saranteas, Kostas, Bakale, Roger

Journal:

IFAC Proceedings Volumes

Year:

2006

Language:

english

File:

PDF, 660 KB

english, 2006

40

ChemInform Abstract: Catalytic Oxidative 1,2-Shift in 1,1′-Disubstituted Olefins Using Arene(iodo)sulfonic Acid as the Precatalyst and Oxone as the Oxidant.

Purohit, Vikram C., Allwein, Shawn P., Bakale, Roger P.

Journal:

Year:

2013

File:

PDF, 30 KB

2013

41

Total Synthesis of [ 14 C]-Labelled Homoharringtonine

Marguerit, Melanie, Little, Gill, Wang, Yi, He, Linli, Allwein, Shawn, Reif, James, Rossi, Jason, Roemmele, Renee, Bakale, Roger

Journal:

European Journal of Organic Chemistry

Year:

2015

Language:

english

File:

PDF, 605 KB

english, 2015

42

An Improved Synthesis of the Free Base and Diglycolate Salt of CEP-33779; A Janus Kinase 2 Inhibitor

Levy, Daniel V., Sclafani, Joseph A., Bakale, Roger P.

Journal:

Organic Process Research & Development

Year:

2016

Language:

english

File:

PDF, 426 KB

english, 2016

43

The First Asymmetric Pilot-Scale Synthesis of TV-45070

Sclafani, Joseph A., Chen, Jian, Levy, Daniel V., Reese, Harlan, Dimitri, Mina, Mudipalli, Partha, Christie, Michael, Neville, Christopher J., Olsen, Mark, Bakale, Roger P.

Journal:

Organic Process Research & Development

Year:

2017

Language:

english

File:

PDF, 1.33 MB

english, 2017

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